Rheological testing

Exploring the flow properties of polymers

Our equipment consisting of rotational and high-pressure capillary rheometers measures rheological properties as a function of temperature, time, and deformation rate. In doing so, viscoelastic properties are investigated in the ranges of small as well as large shear and strain rates. We draw on our experience with a wide variety of polymer materials such as homopolymers, polymer blends, nanocomposites, block copolymers, and compounds.

Contact: Ute Kuhn
Phone: +49 921 55 7475
E-mail: ute.kuhn@uni-bayreuth.de

The Rheometer MCR 702 with TwinDrive technology and two separate motors drives enables the following test modes:

  • 2 EC Modus: both motors can operate as drive units and torque transducer and can be used in different modes: Counter-rotation or SMT-Mode (“Separate Motor Transducer)
  • EC-Mode: only one motor is used (single motor operation)

Max. Frequency ω [rad/s] 628

Angular Velocity [rad/s] 10-9 – 314

Max. Torque [mNm] 230

Min. Torque Rotation [nNm] 1 / 5 (SMT)

Min. Torque Oscillation [nNm] 0.5 / 1 (SMT)

Torque Sensitivity [nNm] 0.1

Normal Force [N] 0.001 – 50

Resolution Normal Force [mN] 0.5

Temperature range [°C] 25 – 450 (Convection Temperature Device)

Features
Pressure cell: 400 bar / 200 °C

UXF-Tool (elongational viscosity)

SRF/TD-Tool (DMTA measurements)

Software
RheoCompass

Location: University of Bayreuth

Contact: Dipl.-Chem.-Ing. Ute Kuhn

Phone: +49 921 55 7475

E-mail: ute.kuhn@uni-bayreuth.de

Maximum angular frequency ω [rad/s] 628

Shear rate [1/s] 0.01 – 100

Maximum torque [mNm] 150.0

Torque resolution [nNm] 0.01

Normal force range [N] 0.05 – 50

Temperature range [°C] 25 – 200

Features
Pressure cell: 400 bar / 200°C

UV curing

Software
RheoCompass

Location: University of Bayreuth

Contact: Dipl.-Chem.-Ing. Ute Kuhn

Phone: +49 921 55 7475

E-mail: ute.kuhn@uni-bayreuth.de

Maximum angular frequency ω [rad/s] 628

Shear rate [1/s] 0.01 – 100

Maximum torque [mNm] 150.0

Torque resolution [nNm] 0.01

Normal force range [N] 0.05 – 50

Temperature range [°C] 25 – 200

Features
Pressure cell: 400 bar / 200°C

Software
RheoPlus, RheoCompass

Property of Neue Materialien Bayreuth GmbH

Location: University of Bayreuth

Contact: Dipl.-Chem.-Ing. Ute Kuhn

Phone: +49 921 55 7475

E-mail: ute.kuhn@uni-bayreuth.de

Maximum angular frequency ω [rad/s] 500

Shear rate [1/s] 0.001 – 100

Torque [nNm] 0.2 – 200.0

Maximum force [N] 50

Angle range [mrad] 0.05 – 500

Temperature range [°C] -150 – 600

Features
Plate – Plate, Cone – Plate, Extensional Viscosity Fixture (EVF), Disposable Plates

Software
TA Orchestrator

Location: University of Bayreuth

Contact: Dipl.-Chem.-Ing. Ute Kuhn

Phone: +49 921 55 7475

E-mail: ute.kuhn@uni-bayreuth.de

The capillary rheometer RG75 can be operated with up to three capillaries simultaneously. This means that the actual viscosity can be determined with relatively little effort. The special coating makes the measuring system suitable for determining the viscosity of corrosive matrices.

Shear rate [mm/s] 0,00004 – 4000

Max. Force [kN] 75

Pressure [ bar] 20 – 2000

Temperature range [°C] 30 – 400

Features
Rheotens 71.97

Laser optics

Location: University of Bayreuth

Contact: M. Sc. Andreas Himmelsbach

Phone: +49 921 55 7462

E-mail: andreas.himmelsbach@uni-bayreuth.de

FURTHER EQUIPMENT AND TECHNOLOGY